Absorption corrections were being applied utilizing SADABS 2014.[40] All non-hydrogen atoms ended up refined anisotropically. Hydrogen atoms ended up assigned to calculated positions utilizing a Using product with correctly mounted isotropic thermal parameters. N-H hydrogens were Positioned and refined with restraints and Together with the U
168 might be rationalized from the loss of the tetrahydropyridine moiety within the dad or mum composition, which gave increase into a radical cation and formation of the methyl fluorophenylacetate species (C9H8FO2•+).
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In the beginning, it absolutely was recognized the two powdered merchandise showed distinct solubility in solvents including methanol and water. As the analyses progressed, it absolutely was recognized that just one merchandise contained the threo
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) enantiomer. As these molecules crystallized in a very centrosymmetric Room team, the inverse enantiomer was also equally existing. The piperidine ring in equally compounds was in the more info chair conformation.
The nitrile intermediate was hydrolysed underneath acidic conditions leading to the formation of the acetamide species. Hydrogenation of your pyridine ring to piperidine adopted, leading to the formation of two racemic erythro
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